Making Dibenzo[a,e]cyclooctene - an Emerging Ligand?
In this video I am synthesizing the ligand dibenzo[a,e[cyclooctene, employing various methods including cold finger sublimation to purify the products!
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Xylene bromination:
Dibenzo[a,e]cyclooctene synthesis:
More information about NBS bromination:
:_Organic_Chemistry_(Smith)/13:_Radical_Reactions/:_Radical_Halogenation_at_an_Allylic_Carbon
–Ziegler_bromination
Synthesis of some complexes with the ligand (where I got structure from):
doi:
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8 months ago 00:15:15 1
Making Dibenzo[a,e]cyclooctene - an Emerging Ligand?